Resume

• 2009

  201 Mullica Hill Road

  Glassboro

  NJ 08028

  Teaching Lecture and Labs. Classes included Chemistry of Everyday Life

  Chem I and II

  Organic Chem. and Adv. Inorg. Chem

  as well as research.

  Assistant Professor

  Rowan University

• 2008

  Schering-Plough Research Institute

  Colonial Chemical Company

  Nova Pharmaceutical Corp

  Rowan University

  Adjunct Professor

  Summit

  NJ

  HPLC method devlopment

  forced degradation studies

  dissolution studies

  Karl-Fisher titrations (for % moisture).

  Analytical Chemist

  Schering-Plough Research Institute

  • General Chemistry Instruction\nResearch Interests:\n• Nitrogen-containing heterocyles\n• Inorganic oxides

  nanomaterials

  and hybrid\nmaterials\n• Characterization by combined inorganic and\norganic methods (NMR

  IR

  MS

  LC-MS

  X-ray\ndiffraction)

  Rowan University

• 2000

  Ph. D.

  Chemistry

• 1991

  Novartis

  Multi-step organic syntheses of drug candidates. Characterization of organic compounds (NMR

  IR

  MS). Chromatography: HPLC

  LC

  TLC. Automated chemistry.

  Novartis

  Research Scientist

  Synthesized and characterized non-natural\nbradykinin mimics. Used computer modeling\n(Polygen Quanta and CHARMm) to design\nisosteres and extract information about bradykinin\nreceptor geometry.

  Nova Pharmaceutical Corp

  Graduate Assistant

  Synthesis and total characterization of ceramic\ntransition metal oxides with low-dimensional\nstructures to understand structure-property\nrelationships in correlated-electron materials\nLouis Whaley\n3\n• Development of air-impermeable coatings (e.g.

  \nSefose-soyate mulls) and inert-atmosphere\ntechniques (e.g.

  Fe3Mo2-O2 buffer pellet) for air-\nsensitive oxides

  Rutgers

  The State University of New Jersey

  Colonial Chemical Company

  Tabernacle

  NJ

  • Special Research Projects Team\no Discover and develop intellectual\nproperty\no Discover new materials to achieve\nresearch goals\no Leverage multidisciplinary expertise in\nproblem-solving\n• New Products Consultation\n• Product Development Troubleshooter

  Contractor

  methods for API and drug product analysis.\n• Instrumentation Includes:\n• Waters Alliance and Agilent HPLC Systems\nUsing:\n• UPLC (Waters Acquity)\n• LC/MS in support of solution-phase

  forced-\ndegradation methods.\n• Moisture Method Development\n• Dissolution Method Development

  Schering Plough

  Scientist I

  (Employment Confirmation Hotline: 1-800-996-7566

  \nemployee number 71764)\n• Skilled in multi-step synthesis and structural\ncharacterization of small-molecule drug\ncandidates.\n• Provider of training to Department scientists

  in\nthe USA and Basel

  Switzerland

  in aspects of\nparallel synthesis/purification (Gilson HPLC\nplatform

  with optional Mass Spec\ndetection/fraction collection): provider of\nequipment maintenance

  upgrade installation

  \nreagent/method development

  and software\noptimization (α-testing).

  Novartis Pharma

  Adjunct Professor

  General Chemistry Instruction\n• Organic Chemistry Instruction\n• Advanced Inorganic Instruction\nResearch Interests:\n• Organic and Inorganic syntheses (vide infra)\nLouis Whaley\n2\n• Thermally-switchable hybrid materials (ionic\nliquids) as reaction solvents

  catalysts

  and\npurification media\no V2O5 nanoparticles by spallation\no Thermochromic hybrid crystals\no M+\nBClF3\n-\n(chlorotrifluoroborate) salts\n• Development of new inorganic reagents to\nshorten organic synthesis schemes\no Thermally switched bromine source\no Double-acceptor synthon\no Polyoxometallate-PEG oxalate\no Indium anilides\n• Parallel/robotic/automated synthesis\n• Design and synthesis of novel antibiotics\no Tethered β-lactam-acrylates

  \nacrylonitriles

  vinyl halides

  Rowan University

  Teaching Assistant

  Graduate teaching experience capitalized on my\nextensive expertise in general chemistry

  \ninstrumental analysis

  organic synthesis and\nproblem solving skills for teaching both small\n(~30 student) and large (~200 student) classes

  Rutgers

  The State University of New Jersey

• 1986

  Ph. D. Degree; Masters Degree

  Synthesis

  Characterization &\nStructure-Property Relationships of Mixed-metal\nOxides/Hybrid Salts

  Masters Degree

  Texas Tech University

• 1982

  Bachelors Degree

  Loyola University

• High-Performance Liquid Chromatography (HPLC)

  Organic Synthesis

  Powder X-ray Diffraction

  FTIR

  TLC

  LC-MS

  Organic Chemistry

  Characterization

  Purification

  NMR

  GC-MS

  Materials Science

  IR

  Gas Chromatography

  Catalysis

  Chemistry

  UV/Vis

  Laboratory

  Inorganic Chemistry

  HPLC

  Autochem: Automated Solution-Phase Parallel Synthesis and Purification via HPLC

  Hanumantha Marepali

  Ruben Tommasi

  Correct order of authors: Tommasi

  Whaley

  Marepali. Summary: Described in this article is \"a practical method for performing parallel solution-phase synthesis with auto- \nmated on-line purification on one HPLC system\" (Autochem). \"The key benefits of \nAutoChem are ease of use

  purity of products

  and facile sample tracking through the use of standard HPLC software for product purification.\" \n

  Autochem: Automated Solution-Phase Parallel Synthesis and Purification via HPLC

  Martha Greenblatt

  Marta Rossell

  Gustaff Van Tendeloo

  Jae-Hyuk Her

  Peter W. Stephens

  Samuel Lofland

  Kandalam V. Ramanujachary

  Mark Croft

  Denis Sheptyakov

  Maxim V. Lobanov

  Sr 3 Fe 5/4 Mo 3/4 O 6.9

  an n=2 Ruddlesden-Popper Phase: Synthesis and properties

  Investigations into mixed-metal oxides reveal correlated-electron behavior in low-dimensional structures. Specifically

  electrically conductive oxides are prepared with magnetic properties that include metal-insulator transitions with respect to temperature changes and changes in applied magnetic fields. These properties are explained on the basis of atomic crystal structure

  magnetic structure

  and existing models of electron transport in crystalline low-dimensional solids.

  Structure-Property Relationships: Synthesis and Characterization of Perovskite-Related Transition-Metal Oxides

  Lei Yu

  Laura Snuffin

  Correct order of authors: Snuffin

  Whaley

  Yu. Abstract: A novel ionic liquid EMIMBF3Cl that contains a BF3Cl− anion has been synthesized. This is the first report of an ionic liquid with a BF3Cl− anion. It was found that CO2 gas can be dissolved and electrochemically reduced at ambient pressure

  and room temperature in the ionic liquid EMIMBF3Cl. The reduction of CO2 occurred at a relatively less negative electrode potential of −1.8 V vs. silver wire

  compared to previous reported values that are between −2.4 and −2.0 V. The reduction current density can be as high as ∼5.7 mA/cm2. The BF3Cl− anion may catalyze the CO2 reduction by forming a Lewis acid-base adduct BF3-CO2.

  Catalytic Electrochemical Reduction of CO2 in Ionic Liquid EMIM BF3Cl.

  Lalita Nohrona-Blob

  James Togo

  James P. Sullivan

  Judith C. Prosser

  Sonya Meeker

  Songfeng Lu

  John P. Carter

  Ron Burch

  Jennifer A. Martin

  Donald J. Kyle

  Additional authors:

  Jaqueline A. Sinsko

  Robert F Walters

  Roger Hiner. \nCorrect order of authors: Kyle

  Martin

  Burch

  Carter

  Lu

  Meeker

  Prosser

  Sullivan

  Togo

  Nohrona-Blob

  Sinsko

  Walters

  Whaley

  Hiner. \nIn some abstracts and citations

  the last few authors are listed as \"et al.\"\nThe hypothesis that a beta-turn in the four C-terminal amino acid residues of bradykinin analogues might be a prerequisite for high receptor affinity is pursued using non-natural amino-acid substitution in oligopeptides modelled after NPC 567. The synthesis of these non-natural amino acids and their incorporation into oligopeptides as well as Ki and pA2 values are reported for 5 decapeptides

  along with conformational mapping of these model peptides. The data was used to better understand the interplay of the conformation of these peptides with the bradykinin receptor.

  Probing the Bradykinin Receptor: Mapping the Geometric Topography Using Ethers of Hydroxyproline in Novel Peptides

  Whaley

  Rowan University

  Novartis Pharma

  Rutgers

  The State University of New Jersey

  Rowan University

  Schering Plough