Good
Professor Kelvin is great! He really cares that we learn the material and he will give out candy to people who ask questions in class. Attendance isn't mandatory but you have to go to class to get lecture notes because he won't post them online. There is also an extra credit group assignment for up to 5% on your final average. Take him. Overall it was a good class.
Texas A&M University College Station - Mechanical Engineering
English
Chinese
French
Doctor of Philosophy (PhD)
Materials Science
University of Sydney
Bachelor of Engineering (B.Eng.)
Biomedical/Medical Engineering
University of Sydney
Bachelor's Degree
Finance
General
University of Sydney
I go to local primary schools and interact with kids in science projects to kindle their interests in science and engineering.
SABES
Nanotechnology
Statistics
Biomedical Engineering
Mathematical Modeling
Spectroscopy
Simulations
Science
Materials Science
Biochemistry
Microscopy
Scanning Electron Microscopy
Characterization
Breaking the icosahedra in boron carbide
Kevin Hemker
Julie Cairney
William Goddard III
Simon Ringer
Takanori Sato
Qi An
Findings of laser-assisted atom probe tomography experiments on boron carbide elucidate an approach for characterizing the atomic structure and interatomic bonding of molecules associated with extraordinary structural stability. The discovery of crystallographic planes in these boron carbide datasets substantiates that crystallinity is maintained to the point of field evaporation
and characterization of individual ionization events gives unexpected evidence of the destruction of individual icosahedra. Statistical analyses of the ions created during the field evaporation process have been used to deduce relative atomic bond strengths and show that the icosahedra in boron carbide are not as stable as anticipated. Combined with quantum mechanics simulations
this result provides insight into the structural instability and amorphization of boron carbide. The temporal
spatial
and compositional information provided by atom probe tomography makes it a unique platform for elucidating the relative stability and interactions of primary building blocks in hierarchically crystalline materials.
Breaking the icosahedra in boron carbide
Simon P Ringer
Julie M Cairney
Peter J Felfer
The current study investigates the strengthening of an Nb-microallyed CASTRIP® steel at 798 K (525 °C) by nitriding in a KNO3 salt bath. Nitriding up to 1 hour dramatically increased the yield strength of the steel by ~35 pct (from 475 to 645 MPa) with no sacrifice of ductility (~16 pct). Further nitriding led to brittle fracture. Hardness profiles of the nitrided steels through the thickness reveal hard surfaces and a relatively softer core. The hardening of the shell in the nitrided steels is thought to be the combined effect of solid solution strengthening from nitrogen and dispersion strengthening from clusters and precipitates. The retained ductility is attributed to the hard-shell–soft-core structure through nitriding.
High Strength and Retained Ductility Achieved in a Nitrided Strip Cast Nb-Microalloyed Steel
Kevin Hemker
Zafir Alam
Pyramidal I slip was observed to be the dominant slip mode in magnesium single crystals compressed quasi-statically along c-axis at room temperature. The slip trace angles resulted from pyramidal I and pyramidal II slips projected on (0 − 1 1 0) and (2 − 1 − 1 0) surfaces were initially calculated
and then measured on 3% deformed magnesium single crystals. The measured angles indicate the prevalence of pyramidal I slip ({10–11}< 11–23 > with the critical resolve shear stress of 54 MPa). The pyramidal slip traces are dense but very fine
suggesting limited < c + a > dislocation activities.
Julie M. Cairney
Simon P. Ringer
David R. Smith
Cluster-strengthened Nb-microalloyed strip cast steels are of interest as clustering during aging leads to an enhancement in strength without compromising ductility
resulting in desirable mechanical properties. However
the precise strengthening mechanism is not well understood. Using in situ heating transmission electron microscopy
clustering was found to impede the movement of dislocations during aging. The attractive combination of ductility and strength was attributed to the effects of recovery and the restricted movement of dislocations through clustering.
The effect of clustering on the mobility of dislocations during aging in Nb-microalloyed strip cast steels: In situ heating TEM observations
The effect of pre-existing defects on the strength and deformation behavior of α-Fe nanopillars
Simon P Ringer
Julie M Cairney
Xiaozhou Liao
Yanbo Wang
Peter J Felfer
Yang Cao
The effects of two types of pre-existing defects
dislocations and clusters
on the strength and deformation behavior of body-centered cubic Fe nanopillars with a diameter of ∼150 nm were investigated using in situ nanocompression in a transmission electron microscope. The plastic deformation of nanopillars containing high initial dislocation densities was observed to be relatively continuous
proceeding via a series of small- and intermediate-scale strain bursts that were associated with the movement/escape of dislocations and the formation of slip bands. Mechanical annealing was observed in nanopillars with high dislocation densities. When the dislocation density was reduced by in situ heating
the nanopillars were much stronger and the plastic deformation behavior transformed to a more abrupt and explosive mode. The introduction of a dispersion of solute atom clusters into nanopillars caused further strengthening as a higher stress level is required for dislocations to pass the clusters. The strengthening effect of cluster dispersion in nanopillars is comparable to that observed in the bulk steel. These phenomena are universal for Fe nanopillars with different crystallographic orientations.
The effect of pre-existing defects on the strength and deformation behavior of α-Fe nanopillars
TEM observations have provided insight into the processing and microstructural evolution of a commercial hot-pressed boron carbide. Fine dispersions of nano-scale AlN precipitates and individual submicron AlN precipitates were observed in a modest fraction of the grains. The nano-precipitates were found to be coherent with a well-defined crystallographic relationship to the matrix. The chemistry
size and distribution of both types of precipitates and the coherency of the nano-precipitates indicate that both intragranular homogeneous and heterogeneous precipitation occurred during cooling.
Precipitation of AlN in a commercial hot-pressed boron carbide
Kevin Hemker
William Goddard III
Rich Haber
Jim McCauley
Fatih Toksoy
Qi An
Recent observations of planar defects in boron carbide have been shown to deviate from perfect mirror symmetry and are referred to as “asymmetric twins.” Here
we demonstrate that these asymmetric twins are really phase boundaries that form in stoichiometric B4C (i.e.
B12C3) but not in B13C2. TEM observations and ab initio simulations have been coupled to show that these planar defects result from an interplay of stoichiometry
atomic positioning
icosahedral twinning
and structural hierarchy. The composition of icosahedra in B4C is B11C and translation of the carbon atom from a polar to equatorial site leads to a shift in bonding and a slight distortion of the lattice. No such distortion is observed in boron-rich B13C2 because the icosahedra do not contain carbon. Implications for tailoring boron carbide with stoichiometry and extrapolations to other hierarchical crystalline materials are discussed.
Atomic-Level Understanding of “Asymmetric Twins” in Boron Carbide
Julie M. Cairney
James G. Williams
Harold Kaul
Simon P. Ringer
This study investigated the microstructure and mechanical properties of Nb-microalloyed ultra-thin cast strip (UCS) steels produced by the CASTRIP® process aged at temperatures below and above the Ac1 temperature (525–800 °C). Aging provided a rapid strength increase without loss in ductility. This is significant because
ordinarily
one of these properties would increase at the expense of the other. Atom probe tomography (APT) and transmission electron microscopy (TEM) revealed that the strengthening was associated with the formation of Nb-rich solute atom clusters and nanoscale precipitates within the microstructure
which retard the movement of dislocations during deformation. The changes in strength and hardness were compared to the microstructural evolution across a range of different aging temperatures and explained in terms of the nucleation kinetics. Cluster-finding algorithms were used to analyse atom probe data
providing quantitative information about the dispersion of these clusters and precipitates. Optimum strengthening was observed where the clusters particles had a radius of 1–2 nm and a volume fraction of 0.027±0.004%.
Cluster strengthening of Nb-microalloyed ultra-thin cast strip steels produced by the CASTRIP® process
Rich A. Haber
Kevin J. Hemker
Luoning Ma
William Rafaniello
Submicrometer boron carbide powders were synthesized using rapid carbothermal reduction (RCR) method. Synthesized boron carbide powders had smaller particle size
lower free carbon
and high density of twins compared to commercial samples. Powders were sintered using spark plasma sintering at different temperatures and dwell times to compare sintering behavior. Synthesized boron carbide powders reached >99% TD at lower temperature and shorter dwell times compared to commercial powders. Improved microhardness observed in the densified RCR samples was likely caused by the combination of higher purity
better stoichiometry control
finer grain size
and a higher density of twin boundaries.
Densification and characterization of rapid carbothermal synthesized boron carbide
Kelvin
Xie
Johns Hopkins University
UNSW Australia
ANSTO
University of Sydney
Texas A&M University
Baltimore
Maryland Area
TEM investigation of defects in Mg and boron carbide to understand their deformation mechanisms.
Assistant Research Scientist
Johns Hopkins University
1. Designed a bio-reactor.\n2. Culture mesenchymal stem cells.
Research Student
Sydney
Australia
UNSW Australia
Using ABAQUS to simulate the thermal stress in power station components.
Research Student Engineer
Sydney
Australia
ANSTO
Bryan/College Station
Texas Area
Assistant Professor
Texas A&M University
1. Prepare optical
SEM and TEM specimens.\n2. Optical
SEM and TEM imaging.\n3. Draft scientific journal papers
Part-time Research Assistant
Sydney
Australia
University of Sydney
In-house TEM expert characterizing chemistry and atomic level defects in Mg and boron carbide.
Post-doctoral Research Fellow
Baltimore
Maryland Area
Johns Hopkins University
A nitrided steel product or thin cast steel strip comprising
by weight
less than 0.25% carbon
between 0.20 and 2.0% manganese
between 0.05 and 0.50% silicon
less than 0.01% aluminum
niobium between 0.01 and about 0.20%
and between 0.01 and 0.075% nitrogen
and having a majority of the microstructure comprised of bainite and acicular ferrite
having more than 70% niobium in solid solution prior to nitriding and having after nitriding for one hour yield strength between 600 MPa and 800 MPa and tensile strength between 650 MPa and 900 MPa and no more than a 2% decrease in total elongation from the steel product prior to nitriding.
Nitriding of niobium steel and product made thereby
US 20120186703 A1
Simon Ringer
Harold Kaul
Chris Killmore
Julie Cairney
Peter Felfer